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Product |
||||||||||
---|---|---|---|---|---|---|---|---|---|---|
% |
% |
|||||||||
Compound |
Crude |
Purified |
B.P. or M.P. |
|||||||
100 |
87 |
B.p. 137°/12 mm. |
||||||||
94 |
90 |
M.p. 54–55° |
||||||||
96 |
86 |
B.p. 154–56°/13 mm. |
||||||||
100 |
91 |
M.p. 55–56° |
||||||||
100 |
80 |
M.p. 50–52° |
||||||||
98 |
90 |
M.p. 94–95° |
||||||||
96 |
.. |
M.p. 62–65° |
||||||||
Appendix
Compounds Referenced (Chemical Abstracts Registry Number)
red phosphorus
ferric and zinc chloride
ethanol (64-17-5)
acetaldehyde (75-07-0)
sulfuric acid (7664-93-9)
acetylene (74-86-2)
hydrochloric acid (7647-01-0)
acetic acid (64-19-7)
ether (60-29-7)
sodium acetate (127-09-3)
aniline (62-53-3)
hydrogen (1333-74-0)
sodium hydroxide (1310-73-2)
formaldehyde (630-08-0)
iron (7439-89-6)
aniline hydrochloride (142-04-1)
tin (7440-31-5)
arsenic acid (1327-52-2)
Raney nickel (7440-02-0)
acetone (67-64-1)
potassium hydroxide (1310-58-3)
zinc (7440-66-6)
palladium (7440-05-3)
Nitrobenzene (98-95-3)
hydriodic acid (10034-85-2)
aluminum oxide (1344-28-1)
Lepidine (491-35-0)
2-Chlorolepidine, chlorolepidine (634-47-9)
2-hydroxy-4-methylquinoline (607-66-9)
β-hydroxyethyl methyl ketone (590-90-9)
2-methyl-4-chloro-6-methoxyquinoline (50593-73-2)
6-Methyllepidine (826-77-7)
8-Methyllepidine (13362-80-6)
2-Methyl-6-methoxyquinoline (1078-28-0)
6-methoxylepidine (41037-26-7)
2-hydroxy-3-cyano-4-methylquinoline
1,2,3,4-tetrahydroquinoline-4-carboxylic acid
4-methylquinoline-2-carboxylic acid
crotonaldehyde (123-73-9)
vinyl methyl ketone, methyl vinyl ketone (78-94-4)
β-chloroethyl methyl ketone (6322-49-2)
1,3,3,-trimethoxybutane (6607-66-5)
1-methoxybutanone-3 (6975-85-5)
paraldehyde (123-53-7)